EN 71-3 2012 [复制链接]

也不知道新的EN 71-3 标准到底进行到什么程度了，翻遍了网络，只找到了最新的Draft的目录，大家将就看看吧（能看到新版的草案中已经给出了有机锡和铬形态分析的具体方法，包括具体要测试的有机锡的种类，等等）。十分期待有人放出全文！ !C)>  
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Foreword vXWESy  
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Introduction 9$w)_RX9W  
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1 Scope <PA$hTYM  
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2 Normative references \V7x3*nA  
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3 Terms and definitions pF{Ri  
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4 Requirements cF6@.)  
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4.1 Categories of toy materials D.JVEKLkU  
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4.1.1 Category I: Dry, brittle, dust-like or pliable material gM:o P.  
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4.1.2 Category II: Liquid or adhesive material AZP >\Dq  
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4.1.3 Category III: material scraped T"lqPbK  
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4.1.4 Categories of different toy materials m$j;FKz+|  
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4.2 Specific Requirements )^xmy6k  
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5 Short Description
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6 Reagents and Equipment =,9'O/br  
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1.6 Reagents ;pYk+r6Cr  
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6.2 Device "=O)2}  
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7 Sampling and Sample Preparation 0cVXUTJ|W  
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7.1 Selection of samples for analysis ':
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7.2 Preparation of standards bv0 %{u&  
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7.3 Sample Preparation 3lqhjA  
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7.3.1 Category I: Dry, brittle, smooth or powdery materials and Category II: Liquid or sticky materials y{<7OTA)  
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7.3.2 Category III: material scraped jn'8F$GU  
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4.7 migration procedures 7pNh|#Uv'  
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7.4.1 General M:~#"lfK  
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7.4.2 Category I: Dry, brittle, smooth or powdery materials and Category II: Liquid or sticky materials px*MOHq K  
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7.4.3 Category III: material scraped t?s1@
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8 Analysis Method B
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8.1 General b@7 ItzD  
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8.2 Chromium (VI) (speciation) G  B15  
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3.8 Organotin |')Z;  
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9 Calculation of results 8 }-"&-X  
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9.1 Standard Elements +~7@K{6q-  
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9.1.1 Calibration Curves 5)0R:  
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9.1.2 Calculation of the concentration ^"l4  
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9.1.3 Evaluation rNdap*.  
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9.2 Chromium (III) and chromium (VI) {um~]  
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9.2.1 Calibration Curves !DXKn\aQf  
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9.2.2 Calculation of the concentration ]hc.cj`\W&  
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9.2.3 Evaluation _=}Efy7  
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3.9 Organotin 5F18/:\n  
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9.3.1 Calibration Curves q{nNWvL  
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9.3.2 Calculation of the migration of individual organotin compounds z1{kZk  
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9.3.3 Calculation of the migration of organotin )v !GiZ"7  
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9.3.4 Evaluation '[Ap/:/UY  
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10 Test report T5H[~b|9-  
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Annex A (informative) Significant technical changes between this European Standard and the previous version Bu7Ztt*  
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Annex B (informative) Results of laboratory proficiency testing - migration of elements (May 2012) w1U2cbCr/  
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Annex C (normative) Requirements for Sieve r:N =?X`N  
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Annex D (informative) Preparation and analysis of the sample im,H|u_f4  
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Annex E (informative) Preparation of standards ?`T0zpC  
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E.1 ICP-MS }^Ymg
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E.1.1 stock solution (M1) [k~}Fe)x  
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E.1.2 Diluted stock solution (M2) |7CFm  
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E.1.3 Work Solutions 1XppC[))
  
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E.2 ICP-OES aam6R/
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E.2.1 stock solution (M1) fbrCl!%P  
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E.2.2 Work Solutions V44M=c7E  
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Annex F (informative) Analysis Method O<>cuW(l  
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F.1 ICP-parameter ;^DG P  
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F.2 method for speciation of chromium #`o]{UfW  
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F.2.1 Scope [4 y7tjar^  
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F.2.2 Summary @<ILF69b  
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F.2.3 reagents B&rw R/d  
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F.2.4 test equipment Wy.^1M/n>~  
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F.2.5 Method -*[:3%  
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F.2.6 reporting X" Upml  
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F.2.7 Example for LC-ICP-MS conditions * zt?y  
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F.3 procedures for organotin 7S2"e[-x  
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F.3.1 Scope A
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F.3.2 terms 3X%h ?DC  
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F.3.3 Summary yoH,4,!G  
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F.3.4 reagents [2PPa
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F.3.5 test equipment Tje(hnN  
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F.3.6 process Sm{> 8e}UE  
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F.3.7 Example for the gas chromatography conditions 3 W%j^nM  
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Annex G (informative) Rationale Sy']fGvx  
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G.1 skin contact (scope) ujzfy  
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G.2 organotin (F.3.7.2) }=}wLm#&1  
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Annex H (informative) Additional information on inspection of certain elements ]jYFrOMy4S  
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Annex ZA (informative) Relationship between this European Standard and the Essential Requirements of EU Directive 2009/48/EC (If (created in due time)) V$sY3,J7A%  
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References ,2^4"gIl