也不知道新的EN 71-3 标准到底进行到什么程度了,翻遍了网络,只找到了最新的Draft的目录,大家将就看看吧(能看到新版的草案中已经给出了有机锡和铬形态分析的具体方法,包括具体要测试的有机锡的种类,等等)。十分期待有人放出全文! x.$1<w64t
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Introduction ; !
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1 Scope 45}v^|Je\
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2 Normative references #Ws53mT
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3 Terms and definitions a&/HSf_G
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4 Requirements rveVCTbC
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4.1 Categories of toy materials =g0*MZ;"
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4.1.1 Category I: Dry, brittle, dust-like or pliable material 2oNV=b[
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4.1.2 Category II: Liquid or adhesive material j:?N!*r=
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4.1.3 Category III: material scraped ;l`X!3
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4.1.4 Categories of different toy materials 8DL h
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4.2 Specific Requirements )T<D6l
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5 Short Description 8 +L7E-
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6 Reagents and Equipment e7hO;=?b'
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1.6 Reagents ,Os7T 1>
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6.2 Device A/hpYa
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7 Sampling and Sample Preparation ./';P<)
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7.1 Selection of samples for analysis 9$:QLE+t
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7.2 Preparation of standards uDpf2(>s
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7.3 Sample Preparation L7i}Ga!8
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7.3.1 Category I: Dry, brittle, smooth or powdery materials and Category II: Liquid or sticky materials #Nu%]
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7.3.2 Category III: material scraped xn%
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4.7 migration procedures +YGw4{\EL
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7.4.1 General M<SbVP|V"
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7.4.2 Category I: Dry, brittle, smooth or powdery materials and Category II: Liquid or sticky materials 1
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8 Analysis Method S:2u3th7
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8.1 General !TV_dKa
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8.2 Chromium (VI) (speciation) -A-hxK*^
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3.8 Organotin V.
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9 Calculation of results ulPrb>i
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9.1 Standard Elements aaf_3UH.B
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9.1.1 Calibration Curves ?CT^Zegmr
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9.1.2 Calculation of the concentration ]}l+ !NV<
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9.1.3 Evaluation P15* VPy
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9.2 Chromium (III) and chromium (VI) syNb0LR
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9.2.1 Calibration Curves W] ;6u
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9.2.2 Calculation of the concentration qQ
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9.2.3 Evaluation F+$@3[Q`N
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3.9 Organotin DF[b?
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9.3.1 Calibration Curves Q
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9.3.2 Calculation of the migration of individual organotin compounds n03SXaU~V
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9.3.3 Calculation of the migration of organotin kGq f@
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9.3.4 Evaluation molowPI
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10 Test report % P)}(e6y
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Annex A (informative) Significant technical changes between this European Standard and the previous version SW'KYzn
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Annex B (informative) Results of laboratory proficiency testing - migration of elements (May 2012) D?F5o^e"h<
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Annex C (normative) Requirements for Sieve w>Sz^_ h
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Annex D (informative) Preparation and analysis of the sample ahv=HWX k
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Annex E (informative) Preparation of standards C$gLi8|m
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E.1 ICP-MS 7Z3qaXPH
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E.1.1 stock solution (M1) GqxK|G1
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E.1.2 Diluted stock solution (M2) 9`&D
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E.1.3 Work Solutions c= uORt>
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E.2 ICP-OES kGP?Jx\PkH
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E.2.2 Work Solutions b87
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Annex F (informative) Analysis Method PV2904
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F.1 ICP-parameter 3Y8
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F.2 method for speciation of chromium d?n~9_9e
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F.2.1 Scope o%a$m9I
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F.2.2 Summary :>k\uW
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F.2.3 reagents
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F.2.4 test equipment >7|37a
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F.2.5 Method Vk"QcW
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F.2.6 reporting C9h8d
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F.2.7 Example for LC-ICP-MS conditions ?@nu]~
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F.3 procedures for organotin ,FTF@h-Cs
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F.3.1 Scope u^ T2
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F.3.2 terms pY2nv/
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F.3.3 Summary Nk
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F.3.4 reagents Y A;S'dxY
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F.3.5 test equipment @]A4{
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F.3.6 process #fa~^]EM]
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F.3.7 Example for the gas chromatography conditions w;X-i.%`
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Annex G (informative) Rationale O10h(Wg
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G.1 skin contact (scope) Q~uj:A]n<
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Annex H (informative) Additional information on inspection of certain elements '%kk&&3'
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Annex ZA (informative) Relationship between this European Standard and the Essential Requirements of EU Directive 2009/48/EC (If (created in due time)) 2,'m]`;GNr
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References zR">'bM: