也不知道新的EN 71-3 标准到底进行到什么程度了,翻遍了网络,只找到了最新的Draft的目录,大家将就看看吧(能看到新版的草案中已经给出了有机锡和铬形态分析的具体方法,包括具体要测试的有机锡的种类,等等)。十分期待有人放出全文! TB>_#+:
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Foreword dEDhdF#f
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Introduction ?*~
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1 Scope bmHj)^v5]
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2 Normative references r`ftflNh(
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3 Terms and definitions @[D5{v)S
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4 Requirements <D
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4.1 Categories of toy materials
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4.1.1 Category I: Dry, brittle, dust-like or pliable material "Ml#,kU<T
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4.1.2 Category II: Liquid or adhesive material [$6YPM>Ee
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4.1.3 Category III: material scraped a U<+ `
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4.1.4 Categories of different toy materials PE_JO(e;Xm
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4.2 Specific Requirements nh+h3"-d
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5 Short Description -LFk7a
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6 Reagents and Equipment L 'e|D=y
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1.6 Reagents }+:X= @Z@
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6.2 Device R,l*@3Q
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7 Sampling and Sample Preparation E,
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7.1 Selection of samples for analysis =|V#~p*
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7.2 Preparation of standards h\|T(597.
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7.3 Sample Preparation 1Uc/r>u9
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7.3.1 Category I: Dry, brittle, smooth or powdery materials and Category II: Liquid or sticky materials x.q "FXu
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7.3.2 Category III: material scraped ZtX
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4.7 migration procedures 2k^'}7G%
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7.4.1 General [$z-
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7.4.2 Category I: Dry, brittle, smooth or powdery materials and Category II: Liquid or sticky materials kG`&Z
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7.4.3 Category III: material scraped Yw_!40`
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8 Analysis Method \J(kM,ZJ
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8.1 General -_XTy!I
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8.2 Chromium (VI) (speciation) qQ8+gZG$R
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3.8 Organotin ]J@-,FFC
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9 Calculation of results 2f620
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9.1 Standard Elements @w`wJ*I4,
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9.1.1 Calibration Curves jFUpf.v2
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9.1.2 Calculation of the concentration 8g
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9.1.3 Evaluation G]4Ca5;Z!N
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9.2 Chromium (III) and chromium (VI) Jv+w{"&
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9.2.1 Calibration Curves =$fz</S=J
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9.2.2 Calculation of the concentration cw
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9.2.3 Evaluation 8hD[z}
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3.9 Organotin %,_ZVgh0
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9.3.1 Calibration Curves e,/]]E/o
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9.3.2 Calculation of the migration of individual organotin compounds r|u[36NmA
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9.3.3 Calculation of the migration of organotin 8%#8P
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9.3.4 Evaluation ]EX6Y
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10 Test report **hQb$
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Annex A (informative) Significant technical changes between this European Standard and the previous version ~Kw#^.$3T
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Annex B (informative) Results of laboratory proficiency testing - migration of elements (May 2012) LgNIb
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Annex C (normative) Requirements for Sieve @Dh2@2`>
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Annex D (informative) Preparation and analysis of the sample )\akIA
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Annex E (informative) Preparation of standards [SPx
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E.1 ICP-MS vF27+/2+R
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E.1.1 stock solution (M1) T}#iXgyx
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E.1.2 Diluted stock solution (M2) QUrPV[JQ
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E.1.3 Work Solutions ]S6Gz/4aV+
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E.2 ICP-OES QN:v4,$d
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E.2.1 stock solution (M1) qRt! kWW
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E.2.2 Work Solutions }9fa]D-a?
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Annex F (informative) Analysis Method UC!mp?
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F.1 ICP-parameter pjeNBSu6
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F.2 method for speciation of chromium H/,KY/>i
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F.2.1 Scope opcanl9pSW
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F.2.2 Summary s QDgNJbU
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F.2.3 reagents {cK<iQJ
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F.2.4 test equipment qCs/sW
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F.2.5 Method ~
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F.2.6 reporting w{ja*F6
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F.2.7 Example for LC-ICP-MS conditions Tmg C {_
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F.3 procedures for organotin x^s,<G
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F.3.1 Scope %
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F.3.2 terms hFV,FBsAO
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F.3.3 Summary #:6-O
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F.3.4 reagents (T1< (YZ
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F.3.5 test equipment eo+<@83
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F.3.6 process TgkVd]4%
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F.3.7 Example for the gas chromatography conditions ny-:%A
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Annex G (informative) Rationale tSHW"R
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G.1 skin contact (scope) @&\Y:aRO%i
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Annex H (informative) Additional information on inspection of certain elements ^_]ZZin
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Annex ZA (informative) Relationship between this European Standard and the Essential Requirements of EU Directive 2009/48/EC (If (created in due time)) -#ZvjEaey
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References _[HZ[ 9c!