EN 71-3 2012 [复制链接]

也不知道新的EN 71-3 标准到底进行到什么程度了，翻遍了网络，只找到了最新的Draft的目录，大家将就看看吧（能看到新版的草案中已经给出了有机锡和铬形态分析的具体方法，包括具体要测试的有机锡的种类，等等）。十分期待有人放出全文！ y42#n  
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Foreword q:]Q% IC^  
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Introduction #&BS ?@  
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1 Scope T1zi0fa'  
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2 Normative references E1(1E?}!  
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3 Terms and definitions kEP<[K  
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4 Requirements >r}Vf9 5[N  
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4.1 Categories of toy materials X| <yq  
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4.1.1 Category I: Dry, brittle, dust-like or pliable material ;J=:IEk  
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4.1.2 Category II: Liquid or adhesive material <'2u a  
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4.1.3 Category III: material scraped ]>8)|]O 6n  
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4.1.4 Categories of different toy materials |!Ists  
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4.2 Specific Requirements ) ,Npv3(  
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5 Short Description xJc.pvVPw  
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6 Reagents and Equipment MYx88y  
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1.6 Reagents w4A#>;Qu*  
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6.2 Device xB,/dMdTj  
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7 Sampling and Sample Preparation }5hZo%w[n  
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7.1 Selection of samples for analysis #/s7\2  
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7.2 Preparation of standards 1q`k}KMy  
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7.3 Sample Preparation T;J7+0  
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7.3.1 Category I: Dry, brittle, smooth or powdery materials and Category II: Liquid or sticky materials A`IHP{aB  
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7.3.2 Category III: material scraped 6N&|2:U  
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4.7 migration procedures )U]:
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7.4.1 General 0e)lY='^_  
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7.4.2 Category I: Dry, brittle, smooth or powdery materials and Category II: Liquid or sticky materials  ccRlql(  
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7.4.3 Category III: material scraped 04P.p6  
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8 Analysis Method 6euR'd^Qi  
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8.1 General Ti hnSb  
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8.2 Chromium (VI) (speciation) ~&t!$  
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3.8 Organotin B0 6s6Q  
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9 Calculation of results 0eQ~#~j&  
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9.1 Standard Elements 6XQ*:N/4al  
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9.1.1 Calibration Curves G> f^2  
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9.1.2 Calculation of the concentration z7O Z4R:  
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9.1.3 Evaluation kvMk :.  
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9.2 Chromium (III) and chromium (VI) zjluX\  
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9.2.1 Calibration Curves 37j\D1Y  
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9.2.2 Calculation of the concentration VxUvvJ{-v  
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9.2.3 Evaluation <GL}1W"Ay  
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3.9 Organotin R`Ys;g/!  
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9.3.1 Calibration Curves  .G5NGB  
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9.3.2 Calculation of the migration of individual organotin compounds |g7nh[  
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9.3.3 Calculation of the migration of organotin ?{@!!te@3v  
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9.3.4 Evaluation xoz*UA
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10 Test report %
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Annex A (informative) Significant technical changes between this European Standard and the previous version R uFu,H-  
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Annex B (informative) Results of laboratory proficiency testing - migration of elements (May 2012) qN`]*baS  
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Annex C (normative) Requirements for Sieve *NwKD:o  
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Annex D (informative) Preparation and analysis of the sample -JyODW#j  
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Annex E (informative) Preparation of standards KbuGf$Bv  
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E.1 ICP-MS hk$nlc|$  
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E.1.1 stock solution (M1) ^%OH}Z`ly  
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E.1.2 Diluted stock solution (M2) \3Ald.EqtM  
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E.1.3 Work Solutions u(G;57ms  
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E.2 ICP-OES {|wTZ  
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E.2.1 stock solution (M1) L$?~TY  
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E.2.2 Work Solutions ..{^"
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Annex F (informative) Analysis Method ?B:wV?-`  
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F.1 ICP-parameter Vk=<,<BB  
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F.2 method for speciation of chromium BnY|t2r  
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F.2.1 Scope Ekp 0.c8:  
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F.2.2 Summary 3ZZI1_j  
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F.2.3 reagents #Jb$AA!z  
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F.2.4 test equipment j0M;2 3@[  
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F.2.5 Method (P_ +m#  
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F.2.6 reporting sIM`Q%  
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F.2.7 Example for LC-ICP-MS conditions %M:"Ai5:  
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F.3 procedures for organotin ^
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F.3.1 Scope kM@,^`&  
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F.3.2 terms u^$ CR  
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F.3.3 Summary {zcjTJ=Zt8  
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F.3.4 reagents 6Xa2A6  
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F.3.5 test equipment +}!eAMQ  
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F.3.6 process "(5}=T@,  
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F.3.7 Example for the gas chromatography conditions LLMkv!%D  
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Annex G (informative) Rationale !(]|!F[m  
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G.1 skin contact (scope) k $);<= ZI  
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G.2 organotin (F.3.7.2) 4bO 7rhve  
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Annex H (informative) Additional information on inspection of certain elements k_skn3,u  
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Annex ZA (informative) Relationship between this European Standard and the Essential Requirements of EU Directive 2009/48/EC (If (created in due time)) OTRTa{TB  
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References V7&L+] !